- PII
- S0023476125040042-1
- DOI
- 10.31857/S0023476125040042
- Publication type
- Article
- Status
- Published
- Authors
- Volume/ Edition
- Volume 70 / Issue number 4
- Pages
- 565-576
- Abstract
- Extended defects in large synthetic diamonds grown at high pressures and high temperatures (HPHT) using thermal gradient method were studied by X-ray topo-tomography with a laboratory setup. It is shown that temperature and growth rate are the principal factors influencing crystalline quality of the diamonds. Synthesis at high temperatures and low rate allows growth of single crystals with low density of dislocations, stacking faults and microtwin lamellae. Annihilation kinetics of the extended defects during annealing at high pressure implies important role of vacancies diffusion. The annihilation of such defects leads to formation of perfect dislocations.
- Keywords
- Date of publication
- 04.04.2025
- Year of publication
- 2025
- Number of purchasers
- 0
- Views
- 12
References
- 1. Palyanov Y., Kupriyanov I., Khokhryakov A., Ralchenko V. // Handbook of Crystal Growth. 2nd ed. / Eds. Nishinaga T., Rudolph P. Amsterdam: Elsevier, 2015. V. 2a. P. 671. https://doi.org/10.1016/B978-0-444-63303-3.00017-1
- 2. D’Haenens-Johansson U.F.S., Butler J.E., Katrusha A.N. // Rev. Miner. Geochem. 2022. V. 88 (1). P. 689. https://doi.org/10.2138/rmg.2022.88.13
- 3. Pal’yanov Yu.N., Borzdov Yu.M., Sokol A.G. et al. // Diamond Relat. Mater. 1998. V. 7. P. 916. https://doi.org/10.1016/S0925-9635 (97)00325-7
- 4. Palyanov Yu.N., Borzdov Yu.M., Gusev V.A. et al. // Nucl. Instrum. Methods Phys. Res. A. 2000. V. 448. P. 179. https://doi.org/10.1016/S0168-9002 (99)00749-4
- 5. Khokhryakov A.F., Palyanov Y.N., Kupriyanov I.N. et al. // J. Cryst. Growth. 2011. V. 317. P. 32. https://doi.org/10.1016/j.jcrysgro.2011.01.011
- 6. Shevyrtalov S., Barannikov A., Palyanov Y. et al. // J. Synchr. Rad. 2021. V. 28. P. 104. https://doi.org/10.1107/S1600577520014538
- 7. Lang A.R. // Diffraction and Imaging Techniques in Material Science / Eds. Amelinckx S. et al. Amsterdam: North Holland, 1978. V. 2. P. 623.
- 8. Moore M., Nailer S.G., Wierzchowski W.K. // Crystals. 2016. V. 6. P. 71. https://doi.org/10.3390/cryst6070071
- 9. Burns R.C., Chumakov A.J., Connell S. et al. // J. Phys. Condens. Matter. 2009. V. 21. P. 364224. https://doi.org/10.1088/0953-8984/21/36/364224
- 10. Kowalski G., Moore M., Gledhill G., Maricic Z. // Diam. Relat. Mater. 1996. V. 4. P. 1254. https://doi.org/10.1016/0925-9635 (96)00540-7
- 11. Пальянов Ю.Н., Хохряков А.Ф., Борздов Ю.М. и др. // Геология и геофизика. 1997. Т. 38 (5). С. 882.
- 12. Palyanov Y.N., Borzdov Y.M., Khokhryakov A.F. et al. // Cryst. Growth Des. 2010. V. 10. P. 3169. https://doi.org/10.1021/cg100322p
- 13. Khokhryakov A.F., Palyanov Y.N. // J. Cryst. Growth. 2006. V. 293. P. 469. https://doi.org/10.1016/j.jcrysgro.2006.05.044
- 14. Khokhryakov A.F., Palyanov Yu.N., Kupriyanov I.N. et al. // J. Cryst. Growth. 2014. V. 386. P. 162. https://doi.org/10.1016/j.jcrysgro.2013.09.047
- 15. Анисимов Н.П., Золотов Д.А., Бузмаков А.В. и др. // Кристаллография. 2023. Т. 68 (4). С. 507. https://doi.org/10.31857/S0023476123600192
- 16. Tolansky S., Miller R.F., Punglia J. // Philos. Mag. 1972. V. 26 (6). P. 1275. https://doi.org/10.1080/14786437208220341
- 17. Frank F.C., Lang A.R., Evans D.J.F. et al. // J. Cryst. Growth. 1990. V. 100. P. 354. https://doi.org/10.1016/0022-0248 (90)90235-D
- 18. Gaukroger M.P., Martineau P.M., Crowder M.J. et al. // Diam. Relat. Mater. 2008. V. 17. P. 262. https://doi.org/10.1016/j.diamond.2007.12.036
- 19. Khokhryakov A.F., Palyanov Y.N. // J. Cryst. Growth. 2007. V. 306. P. 458. https://doi.org/10.1016/j.jcrysgro.2007.05.028
- 20. Tolansky S. // Proc. Roy. Soc. London. A. 1962. V. 270 (1343). P. 443. https://doi.org/10.1098/rspa.1962.0236
- 21. Schindelin J., Arganda-Carreras I., Frise E. et al. // Nat. Methods. 2012. V. 9. P. 676. https://doi.org/10.1038/nmeth.2019
- 22. Martineau P.M., Gaukroger M.P., Guy K.B. et al. // J. Phys.: Condens. Matter 2009. V. 21. P. 364205. https://doi.org/10.1088/0953-8984/21/36/364205
- 23. Masuya S., Hanada K., Oshima T. et al. // Diam. Relat. Mater. 2017. V. 75. P. 155. https://doi.org/10.1016/j.diamond.2017.04.003
- 24. Анцыгин В.Д., Гусев В.А., Калинин А.А. и др. // Автометрия. 1998. № 1. С. 10.
- 25. Tatsumi N., Tamasaku K., Ito T., Sumiya H. // J. Cryst. Growth. 2017. V. 458. P. 27. https://doi.org/10.1016/j.jcrysgro.2016.10.033
- 26. Sumiya H., Harano K., Tamasaku K. // Diam. Relat. Mater. 2015. V. 58. P. 221. https://doi.org/10.1016/j.diamond.2015.08.006
- 27. Квасница В.Н., Харькив А.Д., Вишневский А.А. и др. // Минералогический журнал. 1980. № 3. С. 40.
- 28. Kvasnytsya V. // Diam. Relat. Mater. 2013. V. 39. P. 89. https://doi.org/10.1016/j.diamond.2013.08.005
- 29. Tolansky S., Sunagawa I. // Nature. 1959. V. 184. P. 1526. https://doi.org/10.1038/1841526a0
