- PII
- 10.31857/S0023476123020200-1
- DOI
- 10.31857/S0023476123020200
- Publication type
- Status
- Published
- Authors
- Volume/ Edition
- Volume 68 / Issue number 2
- Pages
- 223-227
- Abstract
- Crystals of the new trigonal borate Ва3Na0.9(OH)1.9[B9O16][B(OH)3] (sp. gr. P31c, a =10.23684(15) Å, c = 8.72926(13) Å) were prepared by the mild hydrothermal synthesis. The filling of the channels in the framework of the polar nonaborate was found to differ from that determined previously. It is consistent with the main features of this structure type with the preservation of sassoline molecules in the channels. The structure contains an additional ОН group, which is involved in the coordination of Ва.
- Keywords
- HYDROTHERMAL SYNTHESIS TRIGONAL POLAR NONABORATE
- Date of publication
- 15.09.2025
- Year of publication
- 2025
- Number of purchasers
- 0
- Views
- 13
References
- 1. The Cambridge Crystallographic Data Centre (CCDC). Inorganic Crystal Structure Data Base – ICSD. https://www.ccdc.cam.ac.uk/, http://www.fiz-karlsruhe.de
- 2. Crystallography Open Database. crystallography.net/cod
- 3. Christ C.L., Clark J.R. // Phys. Chem. Miner. 1977. V. 2. P. 59.
- 4. Liu L., Su X., Yang Y. et al. // Dalton Trans. 2014. V. 43. P. 8905.
- 5. Smith R.W., Keszler D.A. // Mater. Res. Bull. 1989. V. 24. P. 725.
- 6. Bubnova R.S., Krivovichev S.V., Filatov S.K. et al. // J. Solid State Chem. 2007. V. 180. P. 596.
- 7. Белоконева Е.Л., Стефанович С.Ю., Димитрова О.В. // Кристаллография. 2012. Т. 57. С. 70.
- 8. Wei Q., Sun L., Zhang J., Yang G.-Y. // Dalton Trans. 2017. V. 46. P. 7911.
- 9. Heyward C., McMillen C.D., Kolis J. // J. Solid State Chem. 2013. V. 203. P. 166.
- 10. Chen X., Wu L., Chang X., Xiao W. // Solid State Sci. 2014. V. 27. P. 47.
- 11. Топникова А.П., Белоконева Е.Л. // Успехи химии. 2019. Т. 88. № 2. С. 204.
- 12. Белоконева Е.Л., Стефанович С.Ю., Димитрова О.В. и др. // Кристаллография. 2009. Т. 54. № 5. С. 860.
- 13. Agilent (2014). CrysAlis PRO. Agilent Technologies Ltd, Yarnton, Oxfordshire, England.
- 14. Sheldrick G.M. // Acta Cryst. A. 2008. V. 64. P. 112.
- 15. Farrugia L.J. // J. Appl. Cryst. 2012. V. 45. P. 849.
- 16. Белоконева Е.Л., Стефанович С.Ю., Борисова Т.А., Димитрова О.В. // Журн. неорган. химии. 2001. Т. 46. С. 1788.
- 17. Sheldrick G.M. // Acta Cryst. C. 2015. V. 71. P. 3.
- 18. Dowty E. ATOMS. Shape Software, Kingsport, Tennessee, USA, 2006.
- 19. Grube H.H. // Fortsch. Mineral. 1981. B. 59. S. 58.
- 20. Lu J., Shi G., Wu H. et al. // RSC Adv. 2017. V. 7. P. 20259.
- 21. Wu Ch., Song J., Li L. et al. // J. Mater. Chem. C. 2016. V. 4. P. 8189.
- 22. Wei Q., Wang J.-J., He Ch. et al. // Chem. Eur. J. Commun. 2016. V. 22. P. 10759.
- 23. Wu Ch., Jiang X., Lin L. et al. // Angew. Chem. Int. Ed. 2021. V. 60. № 52. P. 27151.
